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separate |
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| After addition of deuterated internal standards, samples were extracted twice with dichloromethane (25 mL each time) for 2 min each with 2 min separation times using 1-L separatory funnels. Small companies and craftsmen specialized in activities as: insulation and roof reconstruction, thermo insulation of buildings, interior design, separatory walls, attics and other similar activities. Each sample was split into four 1-L fractions in 2-L glass separatory funnels. |
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